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Solvent Systems for Trituration









EtOAc

Solvent System Examples Comments
EtOAc 100% EtOAc   [see procedure]
100% EtOAc   [see procedure]
100% EtOAc   [see procedure]
100% EtOAc   [see procedure]
100% EtOAc   [see procedure]
--
EtOAc/hexane -- --
EtOAc/heptane 10% EtOAc/heptane   [see procedure] --
EtOAc/PE 30:1 PE/EtOAc   [see procedure]
1:1 PE/EtOAc   [see procedure]
--

DCM

Solvent System Examples Comments
DCM 100% DCM   [see procedure] --
DCM/hexane DCM/hexane   [see procedure] --
DCM/heptane -- --

ether

Solvent System Examples Comments
ether 100% ether   [see procedure]
100% ether   [see procedure]
100% ether   [see procedure]
100% ether   [see procedure]
100% ether   [see procedure]
--
ether/hexane 1:5 ether/hexane   [see procedure] --
ether/heptane 2:1 ether/heptane   [see procedure] --

MTBE

Solvent System Examples Comments
MTBE 100% MTBE   [see procedure] --
MTBE/hexane MTBE/hexane   [see procedure] --
MTBE/heptane 10% MTBE/heptane   [see procedure] --

THF

Solvent System Examples Comments
THF 100% THF   [see procedure] --

MeOH

Solvent System Examples Comments
MeOH 100% MeOH   [see procedure] --
MeOH/EtOAc 10% MeOH/EtOAc   [see procedure] --
MeOH/H2O 5:6 MeOH/H2O   [see procedure] --

EtOH

Solvent System Examples Comments
EtOH 100% EtOH   [see procedure] --
EtOH/H2O -- --

IPA

Solvent System Examples Comments
IPA -- --

hexane

Solvent System Examples Comments
hexane 100% hexane   [see procedure]
100% hexane   [see procedure]
100% hexane   [see procedure]
--

heptane

Solvent System Examples Comments
heptane -- --

pentane

Solvent System Examples Comments
pentane 100% pentane   [see procedure]
100% pentane   [see procedure]
100% pentane   [see procedure]
--

PE

Solvent System Examples Comments
PE 100% PE   [see procedure] --

ACN

Solvent System Examples Comments
ACN -- --

H2O

Solvent System Examples Comments
H2O 100% H2O   [see procedure] --